Thiophosphate ion
HPLC Analysis of Polar Environmental Contaminants on Amaze HD Mixed-Mode Column with LC/MS Compatible Conditions
Conditions of Experiment
| Column: | Amaze HD |
| Separation Modes: | HILIC, cation-exchange, anion-exclusion |
| Column Dimenstions: | 4.6x150 mm, 3 μm, 100A |
| Mobile Phase: | 78% ACN with 44 mM AmFm pH 3 |
| Detection: | Corona CAD |
| Sample: | 0.3 mg/ml |
| Injection: | 2 μL |
| Flow rate: | 1 ml/min |
Analytes
| Class of compounds: | Inorganic acid, Inorganic anion, Inorganic cation, Organic acid |
| Nature of compounds: | Acidic, Basic, Hydrophilic, Polar |
| Compounds: | Perchlorate ion, Chlorate ion, Bromide ion, Thiophosphate ion, Ethylphosphonate ion, Phosphonate ion, Potassium ion, Sodium ion, Phosphate Ion |
Separation of Phosphate, Thiophosphate and Sodium Ions on Amaze TH Column
Conditions of Experiment
| Column: | Amaze TH |
| Separation Modes: | HILIC, cation-exchange, anion-exchange |
| Column Dimenstions: | 3.0x100 mm, 3 um, 100A |
| Mobile Phase: | 75% ACN with 30 mM AmFm pH 3 |
| Detection: | ELSD, 45°C |
| Sample: | 0.5-0.8 mg/ml |
| Injection: | 10 uL |
| Flow rate: | 0.6 ml/min |
Analytes
| Class of compounds: | Inorganic acid, Inorganic anion, Inorganic cation |
| Nature of compounds: | Acidic, Basic, Hydrophilic, Polar |
| Compounds: | Thiophosphate ion, Phosphate Ion, Sodium ion |
Separation of Phosphate, Thiophosphate and Sodium Ions on Amaze HA Column
Conditions of Experiment
| Column: | Amaze HA |
| Separation Modes: | HILIC, cation-exclusion, anion-exchange |
| Column Dimenstions: | 4.6x50 mm, 3 um, 100A |
| Mobile Phase: | 30% ACN with 10 mM AmFm pH 3 |
| Detection: | 0.5-0.8 mg/ml |
| Sample: | ELSD, 45°C |
| Injection: | 10 uL |
| Flow rate: | 1 ml/min |
Analytes
| Class of compounds: | Inorganic acid, Inorganic anion, Inorganic cation |
| Nature of compounds: | Acidic, Basic, Hydrophilic, Polar |
| Compounds: | Thiophosphate ion, Phosphate Ion, Sodium ion |
